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March 10, 2010
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Alumina, Activity Super I Minimize
 
 
Alumina, Activity Super I is designed for the separation of polar samples in non-solvent systems as well as the purification and dehydration of solvents. In a non-polar environment Super I shows sorption capacity approximately twice as high as Activity I. Alumina Activity Super I has residual water content of 1 /- 0.1% and its specific surface area is ~200 m2/g.  The high activity level lends itself to the separation of polar samples in nonpolar solvent systems, specifically, the purification of solvents.
 

Deactivation of Alumina, Activity Super I:

Deactivation allows the chromatographer the flexibility and freedom to deactivate alumina to the precise activity level required for their specific application.  Sorbent Technologies' standardized aluminas are based on a deactivation scale (see chart.)  The deactivation procedure holds true for all three pH levels (Acid, Neutral, Basic.)  These three surface types show an identical initial activity and when deactivated with identical volumes of deactivator (e.g. water) they exhibit the identical lower activity statuses.  The percent of water addition is based upon weight/weight relationships.  Activity level is according to Brockmann.

 
Activity

Super I

I

II

III

IV

V

% water to add

0

1

4

7

10

19

 

Alumina

pH

Activity

Loss on Ignition approx.

Distribution

Water Sol. Matter approx.

Bulk Density approx.

Surface Area approx.

Acid

4.5

Super I

1.3 %

50-200µm

0.1 %

0.8 g/ml

200 m2/g

Neutral

7.5

Super I

1 %

50-200µm

0.1 %

0.8 g/ml

200 m2/g

Basic

10

Super I

1 %

50-200µm

0.1 %

0.8 g/ml

200 m2/g

 

Typical Applications for Super I Aluminas

Acid

Neutral

Basic 

Food dyestuffs Ketosteroids Purification of organic solvents
determination of morphine Glycosides Synthetic bases
determination of diphenyl Vitamins Dehydration of ethers
  Removal of pyrogens Removal of peroxides
  Dehydration of organic solvents Natural and synthetic dyestuffs
  Alkaloids Hydrocarbons

 

Deactivation Procedure:

  1. Weigh a known quantity of alumina and place into a tightly sealed vessel.
  2. Add the required amount of water (by weight or volume.)
  3. Shake the mixture in the closed vessel until all lumps disappear.
  4. Allow the mixture to cool (preferably overnight.)
  5. The container should remain tightly closed to retain activity level and can be stored for later use.
Available Products Minimize
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Alumina, Acid, Super I, 50-200um, 500g Product Information 

Cat. # 15100-05
Qty. 500 g
Price $92.95
  
Alumina, Acid, Super I, 50-200um, 1kg Product Information 

Cat. # 15100-1
Qty. 1 kg
Price $220.00
  
Alumina, Acid, Super I, 50-200um, 5kg Product Information 

Cat. # 15100-5
Qty. 5 kg
Price $643.50
  
Alumina, Acid, Super I, 50-200um, 50kg Product Information 

Cat. # 15100-50
Qty. 50 kg
Price $3,300.44
  
Alumina, Neutral, Super I, 50-200um, 500g Product Information 

Cat. # 15130-05
Qty. 500 g
Price $92.95
  
Alumina, Neutral, Super I, 50-200um, 1kg Product Information 

Cat. # 15130-1
Qty. 1 kg
Price $220.00
  
Alumina, Neutral, Super I, 50-200um, 5kg Product Information 

Cat. # 15130-5
Qty. 5 kg
Price $643.50
  
Alumina, Neutral, Super I, 50-200um, 50kg Product Information 

Cat. # 15130-50
Qty. 50 kg
Price $3,300.44
  
Alumina, Basic, Super I, 50-200um, 500g Product Information 

Cat. # 15160-05
Qty. 500 g
Price $92.95
  
Alumina, Basic, Super I, 50-200um, 1kg Product Information 

Cat. # 15160-1
Qty. 1 kg
Price $220.00
  
Alumina, Basic, Super I, 50-200um, 5kg Product Information 

Cat. # 15160-5
Qty. 5 kg
Price $643.50
  
Alumina, Basic, Super I, 50-200um, 50kg Product Information 

Cat. # 15160-50
Qty. 50 kg
Price $3,300.44